{"id":52,"date":"2021-06-14T11:23:52","date_gmt":"2021-06-14T15:23:52","guid":{"rendered":"https:\/\/sites.bu.edu\/cheminst\/?page_id=52"},"modified":"2025-09-11T16:55:55","modified_gmt":"2025-09-11T20:55:55","slug":"cic-nmr-reservation","status":"publish","type":"page","link":"https:\/\/sites.bu.edu\/cheminst\/nuclear-magnetic-resonance\/cic-nmr-reservation\/","title":{"rendered":""},"content":{"rendered":"<h2>NMR\u00a0Reservations<\/h2>\n<p>&nbsp;<\/p>\n<p><img loading=\"lazy\" src=\"\/cheminst\/files\/2021\/05\/NMRHeaderImage-636x159.jpg\" alt=\"\" width=\"636\" height=\"159\" class=\"alignnone size-medium wp-image-21\" srcset=\"https:\/\/sites.bu.edu\/cheminst\/files\/2021\/05\/NMRHeaderImage-636x159.jpg 636w, https:\/\/sites.bu.edu\/cheminst\/files\/2021\/05\/NMRHeaderImage.jpg 650w\" sizes=\"(max-width: 636px) 100vw, 636px\" \/><\/p>\n<h3>To reserve time on the v400, m500 and b600 NMR spectrometers, please click here<span style=\"color: #ff0000;\">\u00a0<a href=\"http:\/\/cic.bu.edu\/cgi-bin\/Calcium40.pl?Op=UserLogin\" style=\"color: #ff0000;\">NMR Reservation Calendar<\/a><\/span><\/h3>\n<p>Your login is your kerberos email username however, the password is<span>\u00a0<\/span><strong>cicnmr06<\/strong><span>\u00a0<\/span>(<em>for example, <strong>name<\/strong>@bu.edu, your login is <strong>name<\/strong><\/em>).<\/p>\n<h4>Before You Begin: Connect to the BU Network<\/h4>\n<p>You must be connected to the BU Network, this can be via the wired network, the wireless network, or remotely via the<span>\u00a0<\/span><a title=\"BU VPN\" href=\"http:\/\/www.bu.edu\/tech\/accounts\/remote\/vpn\/\" target=\"_blank\" rel=\"noopener noreferrer\">BU VPN<\/a>. You must be connected to the network to access the reservation calendar.<\/p>\n<h3><strong>Reservation Policies:<\/strong><\/h3>\n<h4><span><strong>Users must follow these rules when reserving time on a spectrometer:<\/strong><\/span><\/h4>\n<ol>\n<li>NMR reservations will be monitored by <strong>Paul Ralifo<\/strong> weekly at the end of each business week (Fridays).<\/li>\n<li>To simplify tracking on NMR reservations, users are required to include their <strong>Lab Name<\/strong> in the <strong>\u201cYour Name and Lab Name\u201d<\/strong> field of the <em>Add New Event\u00a0<\/em>pop up window of the Calendar.<\/li>\n<li>If you need extra time than is allowed on any spectrometer (DayQ or NightQ)contact Paul Ralifo first to get approval.<\/li>\n<li>Reservation rules for each NMR are further explained below.<\/li>\n<\/ol>\n<h4><strong>Policy for reservation offenders:<\/strong><\/h4>\n<ol>\n<li>First time offenders will get an email warning. CIC Instrument committee chair will be copied on the email.<\/li>\n<li>Second time offenders will have their NMR privileges revoked for one week. User\u2019s PI and Chemistry\u2019s Director of Operations will also be notified.<\/li>\n<li>Third time offenders and thereafter will have their NMR privileges revoked for one month. User\u2019s PI, Chemistry\u2019s Director of Operations, and Department Chair will also be notified.<\/li>\n<\/ol>\n<h2><span><b><span size=\"4\">v400:<\/span><\/b><\/span><\/h2>\n<p><span style=\"color: #ff0000;\">You must reserve this NMR every time you want to use it!!!<\/span><\/p>\n<p><b>TIME PERIODS FOR NMR RESERVATION<\/b><\/p>\n<table>\n<tbody>\n<tr>\n<td>M-F:<\/td>\n<td><b>8:00am-6:00pm<\/b><\/td>\n<td><strong><span style=\"color: #ff0000;\">30 mins<\/span><\/strong> max<\/td>\n<\/tr>\n<tr>\n<td><\/td>\n<td><b>6:00pm-8:00pm<\/b><\/td>\n<td><strong><span style=\"color: #ff0000;\">1 hour<\/span><\/strong> max<\/td>\n<\/tr>\n<tr>\n<td><\/td>\n<td><b>8:00pm-8:00am<\/b><\/td>\n<td>Overnight<\/td>\n<\/tr>\n<tr>\n<td>Sat-Sun:<\/td>\n<td><b>8:00am-7:00pm<\/b><\/td>\n<td><strong><span style=\"color: #ff0000;\">30 mins<\/span><\/strong> max<\/td>\n<\/tr>\n<tr>\n<td><\/td>\n<td><b>7:00pm-8:00am<\/b><\/td>\n<td>Overnight<\/td>\n<\/tr>\n<\/tbody>\n<\/table>\n<p><b>SIGN-UP RULES\u00a0<\/b><\/p>\n<ol>\n<li>Overnight Reservation rules will reset on each Monday and reservations can be made up to 7 days in advance. Overnight reservations are made by rotating through\u00a0each lab group- any one particular group cannot book more than one overnight per machine (SHARE!). If the Overnight time is still unreserved, by 5pm on that day, the\u00a0time can be reserved by any authorized user, even if he\/she has already used Overnight time that week.<\/li>\n<li>Maximum time slots for each of the NMRs at particular times are listed above. Each research group can only reserve a maximum of two consecutive non-overnight time slots per spectrometer. For\u00a0example, a user can only reserve the 400 NMR on weekdays for a maximum of 30 mins between 8am and 6pm and the same group can make two consecutive reservations to a maximum of 60 mins for this\u00a0instrument. CONSECUTIVE TIME SLOTS CANNOT BE RESERVED BY THE SAME PERSON!<\/li>\n<li>Every user must reserve time on the 400 MHz NMR before using the instrument. Any user that is caught using the 400 without reserving time may have their experiments aborted by users who have reserved the time on the Calendar.<\/li>\n<li>Reserved time that is not needed should be canceled ASAP. If you cannot make your reserved time slot less than an hour in advance please email the\u00a0<a href=\"mailto:chem-nmrusers-list@bu.edu\">chem-nmrusers-list@bu.edu<\/a>\u00a0and let people know that\u00a0the time slot is available for use.<\/li>\n<li>Parallel booking of more than one spectrometer is strictly prohibited.<\/li>\n<li>Users who run experiments during time booked by someone else without that person\u2019s permission or, who reserve instruments under another user\u2019s name to sidestep the rules will be banned\u00a0from using the NMRs.<\/li>\n<li>Users who run experiments during time booked by someone else without that person\u2019s permission or, who reserve instruments under another user\u2019s name to sidestep the rules will be banned\u00a0from using the NMRs.<\/li>\n<\/ol>\n<h2><b><span size=\"4\">m500:<\/span><\/b><\/h2>\n<p><span style=\"color: #ff0000;\">No reservations needed for DayQ. Must reserve NightQ slots in advance!!!<\/span><\/p>\n<p><b>TIME PERIODS FOR NMR RESERVATION<\/b><\/p>\n<table width=\"495\" style=\"font-weight: 400;\" height=\"209\">\n<tbody>\n<tr>\n<td rowspan=\"3\"><strong>DayQ:<\/strong><\/p>\n<p><span style=\"color: #ff0000;\">15mins max per sample<\/span><\/td>\n<td><strong>M-F<\/strong><\/td>\n<td><strong>\u00a09:00 AM \u2013 9:00 PM<\/strong><\/td>\n<\/tr>\n<tr>\n<td><strong>Sat<\/strong><\/td>\n<td><strong>9:00 AM \u2013 7:00 PM<\/strong><\/td>\n<\/tr>\n<tr>\n<td><strong>Sun<\/strong><\/td>\n<td><strong>9:00 AM \u2013 4:00 PM<\/strong><\/td>\n<\/tr>\n<tr>\n<td rowspan=\"3\"><strong>NightQ:<\/strong><\/p>\n<p>&nbsp;<\/td>\n<td><strong>M-F:<\/strong><\/td>\n<td><strong>9:00 PM \u2013 9:00 AM,<\/strong><\/td>\n<\/tr>\n<tr>\n<td><strong>Sat:<\/strong><\/td>\n<td><strong>7:00 PM \u2013 9:00 AM<\/strong><\/td>\n<\/tr>\n<tr>\n<td><strong>Sun:<\/strong><\/td>\n<td><strong>4:00 PM \u2013 9:00 AM<\/strong><\/td>\n<\/tr>\n<\/tbody>\n<\/table>\n<p style=\"font-weight: 400;\"><strong>SIGN-UP RULES:<\/strong><\/p>\n<ol style=\"font-weight: 400;\">\n<li>Overnight (O\/N) Reservation rules will reset on each Monday morning and reservations can be made up to 7 days in advance. O\/N reservations are made by rotating through each research group; each research group can only reserve <strong><u>one\u00a0O\/N per week<\/u> <\/strong>except\u00a0the following:\n<ul>\n<li>If on that day (from Monday to Friday) the nightQ is not reserved by 5 PM, then that NightQ slot is up for grabs. On Saturdays and Sundays, the\u00a0NightQ is up for grabs at 4:00 and 12:00 PM respectively if still unreserved.<\/li>\n<li>If there is remaining NightQ time available (after the Primary NightQ User\u2019s reservation) by 5PM. <strong>The primary nightQ user is the first user to reserve\u00a0nightQ time for that day<\/strong>.<\/li>\n<li>Prior approval from Paul Ralifo.<\/li>\n<\/ul>\n<\/li>\n<li>When reserving the NightQ, <strong>only reserve the time you need<\/strong> and not the whole nightQ slot, i.e. if you will only be using 3 hours to\u00a0run a\u00a0<sup>13<\/sup>C NMR, you should only reserve from 9:00 PM \u2013 12:00 AM (and not 9:00 PM \u2013 9:00 AM). This will allow other users the chance to make use of the remaining nightQ.<\/li>\n<li>Remaining NightQ time can be reserved at 5:00 PM (or 4:00 PM on Saturdays and 12:00 PM on Sundays).\u00a0You must reserve time on the Calendar to use the nightQ.<\/li>\n<li>Overnight Reservations for the week start on Monday at 9:00 AM.<\/li>\n<li>NightQ samples cannot be queued before 5 PM.<\/li>\n<li><strong>For dayQ, users are asked to limit the amount of time (for all samples queued in a row) to less than 30 minutes.<\/strong> For example, if you need to run 4 x 15 mins Carbon experiments, do not queue all 4 samples at once but break them up to allow others to be able to run samples in a decent amount of time.<\/li>\n<\/ol>\n<p>&nbsp;<\/p>\n<h2><b><span size=\"4\">b600:<\/span><\/b><\/h2>\n<p><span style=\"color: #ff0000;\">No reservations needed for DayQ. Must reserve NightQ slots in advance!!!<\/span><\/p>\n<p><b>TIME PERIODS FOR NMR RESERVATION<\/b><\/p>\n<table width=\"495\" style=\"font-weight: 400;\" height=\"209\">\n<tbody>\n<tr>\n<td rowspan=\"3\"><strong>DayQ:<\/strong><\/p>\n<p><span style=\"color: #ff0000;\">30mins max per sample<\/span><\/td>\n<td><strong>M-F<\/strong><\/td>\n<td><strong>\u00a08:00 AM \u2013 8:00 PM<\/strong><\/td>\n<\/tr>\n<tr>\n<td><strong>Sat<\/strong><\/td>\n<td><strong>8:00 AM \u2013 8:00 PM<\/strong><\/td>\n<\/tr>\n<tr>\n<td><strong>Sun<\/strong><\/td>\n<td><strong>8:00 AM \u2013 8:00 PM<\/strong><\/td>\n<\/tr>\n<tr>\n<td rowspan=\"3\"><strong>NightQ:<\/strong><\/p>\n<p>&nbsp;<\/td>\n<td><strong>M-F:<\/strong><\/td>\n<td><strong>8:00 PM \u2013 8:00 AM,<\/strong><\/td>\n<\/tr>\n<tr>\n<td><strong>Sat:<\/strong><\/td>\n<td><strong>8:00 PM \u2013 8:00 AM<\/strong><\/td>\n<\/tr>\n<tr>\n<td><strong>Sun:<\/strong><\/td>\n<td><strong>8:00 PM \u2013 8:00 AM<\/strong><\/td>\n<\/tr>\n<\/tbody>\n<\/table>\n<p style=\"font-weight: 400;\"><strong>SIGN-UP RULES:<\/strong><\/p>\n<ol style=\"font-weight: 400;\">\n<li>Overnight (O\/N) Reservation rules will reset on each Monday morning and reservations can be made up to 7 days in advance. O\/N reservations are made by rotating through each research group; each research group can only reserve <strong><u>one\u00a0O\/N per week<\/u> <\/strong>except\u00a0the following:\n<ul>\n<li>If on that day (from Monday to Friday) the nightQ is not reserved by 5 PM, then that NightQ slot is up for grabs. On Saturdays and Sundays, the\u00a0NightQ is up for grabs at 4:00 and 12:00 PM respectively if still unreserved.<\/li>\n<li>If there is remaining NightQ time available (after the Primary NightQ User\u2019s reservation) by 5PM. <strong>The primary nightQ user is the first user to reserve\u00a0nightQ time for that day.<\/strong><\/li>\n<li>Prior approval from Paul Ralifo.<\/li>\n<\/ul>\n<\/li>\n<li>When reserving the NightQ, <strong>only reserve the time you need<\/strong> and not the whole nightQ slot, i.e. if you will only be using 3 hours to\u00a0run a\u00a0<sup>13<\/sup>C NMR, you should only reserve from 8:00 PM \u2013 11:00 pM (and not 8:00 PM \u2013 8:00 AM). This will allow other users the chance to make use of the remaining nightQ.<\/li>\n<li>Remaining NightQ time can be reserved at 5:00 PM (or 4:00 PM on Saturdays and 12:00 PM on Sundays).\u00a0You must reserve time on the Calendar to use the nightQ.<\/li>\n<li>Overnight Reservations for the week start on Monday at 8:00 AM.<\/li>\n<li>NightQ samples cannot be queued before 3 PM.<\/li>\n<li><strong>For dayQ, users are asked to limit the amount of time (for all samples queued in a row) to less than 30 mins.<\/strong> For example, if you need to run 2 x 30 mins Carbon experiments, do not queue all samples at once but break them up to allow others to be able to run samples in a decent amount of time.<\/li>\n<\/ol>\n<p><b>TAKE WHAT YOU NEED AND NO MORE. USE ALL YOU TAKE<\/b><\/p>\n<p><strong>If you run into any problems making reservations please contact Paul Ralifo<a href=\"mailto:ralifo@bu.edu\"><\/a>\u00a0as soon as possible.<\/strong><\/p>\n","protected":false},"excerpt":{"rendered":"<p>NMR\u00a0Reservations &nbsp; To reserve time on the v400, m500 and b600 NMR spectrometers, please click here\u00a0NMR Reservation Calendar Your login is your kerberos email username however, the password is\u00a0cicnmr06\u00a0(for example, name@bu.edu, your login is name). Before You Begin: Connect to the BU Network You must be connected to the BU Network, this can be via [&hellip;]<\/p>\n","protected":false},"author":10766,"featured_media":0,"parent":20,"menu_order":1,"comment_status":"closed","ping_status":"closed","template":"","meta":[],"_links":{"self":[{"href":"https:\/\/sites.bu.edu\/cheminst\/wp-json\/wp\/v2\/pages\/52"}],"collection":[{"href":"https:\/\/sites.bu.edu\/cheminst\/wp-json\/wp\/v2\/pages"}],"about":[{"href":"https:\/\/sites.bu.edu\/cheminst\/wp-json\/wp\/v2\/types\/page"}],"author":[{"embeddable":true,"href":"https:\/\/sites.bu.edu\/cheminst\/wp-json\/wp\/v2\/users\/10766"}],"replies":[{"embeddable":true,"href":"https:\/\/sites.bu.edu\/cheminst\/wp-json\/wp\/v2\/comments?post=52"}],"version-history":[{"count":32,"href":"https:\/\/sites.bu.edu\/cheminst\/wp-json\/wp\/v2\/pages\/52\/revisions"}],"predecessor-version":[{"id":577,"href":"https:\/\/sites.bu.edu\/cheminst\/wp-json\/wp\/v2\/pages\/52\/revisions\/577"}],"up":[{"embeddable":true,"href":"https:\/\/sites.bu.edu\/cheminst\/wp-json\/wp\/v2\/pages\/20"}],"wp:attachment":[{"href":"https:\/\/sites.bu.edu\/cheminst\/wp-json\/wp\/v2\/media?parent=52"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}