{"id":216,"date":"2021-06-17T14:38:02","date_gmt":"2021-06-17T18:38:02","guid":{"rendered":"https:\/\/sites.bu.edu\/cheminst\/?page_id=216"},"modified":"2023-08-22T09:58:57","modified_gmt":"2023-08-22T13:58:57","slug":"data-access","status":"publish","type":"page","link":"https:\/\/sites.bu.edu\/cheminst\/nuclear-magnetic-resonance\/data-access\/","title":{"rendered":""},"content":{"rendered":"<h2>NMR Data Access<\/h2>\n<p><img loading=\"lazy\" src=\"\/cheminst\/files\/2021\/05\/NMRHeaderImage-636x159.jpg\" alt=\"\" width=\"636\" height=\"159\" class=\"alignnone size-medium wp-image-21\" srcset=\"https:\/\/sites.bu.edu\/cheminst\/files\/2021\/05\/NMRHeaderImage-636x159.jpg 636w, https:\/\/sites.bu.edu\/cheminst\/files\/2021\/05\/NMRHeaderImage.jpg 650w\" sizes=\"(max-width: 636px) 100vw, 636px\" \/><\/p>\n<div style=\"text-align: justify;\">\n<h2><\/h2>\n<h4><span style=\"color: #008000;\">NOTE: if accessing from off campus you must connect via BU&#8217;s <a href=\"https:\/\/www.bu.edu\/tech\/services\/cccs\/remote\/vpn\/\" style=\"color: #008000;\">off-campus VPN<\/a>.<\/span><\/h4>\n<h3>1. All the CIC NMR data is being saved directly to the casfs.bu.edu server.<\/h3>\n<p>Each instrument has its own share on the server. On the NMR host computers, the data will appear on the shares that were mounted as follows:<\/p>\n<ul>\n<li><strong>500 MHz NMR<\/strong>: you can find your data in <span style=\"color: blue;\">\/mnt\/cic_m500<\/span><\/li>\n<li><strong>400 MHz NMR<\/strong>: you can find your data in <span style=\"color: blue;\">\/mnt\/cic_v400<\/span><\/li>\n<li><strong>600 MHz NMR:<\/strong> you can find your data in <span style=\"color: #0000ff;\">z:cic\\b600<\/span><\/li>\n<\/ul>\n<p>Here, you can navigate to your folder, and find your NMR data. <span style=\"color: red;\">You will not find your NMR data in the \/home\/walkupX\/vnmrsys\/data directory as you used to before.<\/span> If you need to access your data on the NMR host computers you will need to navigate to the <span style=\"color: blue;\">\/mnt<\/span> directory. Because your data is being saved directly on the casfs.bu.edu server, your data will be available immediately on the server shares and you can access them from your computers. You can map the shares according to the instructions below.<\/p>\n<h3>2. To connect to the shares:<\/h3>\n<h4 style=\"color: blue;\">Windows:<\/h4>\n<ol>\n<li><strong>400 NMR<\/strong>: map a network drive to <span style=\"color: blue;\">\\\\casfs.bu.edu\\cic v400<\/span> (there is a space between cic and v400) . You will be asked to login: in the username field enter AD\\your-BU-Kerberos-username and then your Kerberos password in the password field. Note that you must add <span style=\"color: blue;\">ad\\<\/span> in front of your username.<\/li>\n<li><strong>500 NMR<\/strong>: map a network drive to <span style=\"color: blue;\">\\\\casfs.bu.edu\\cic m500<\/span> (there is a space between cic and m500) . You will be asked to login: in the username field enter AD\\your-BU-Kerberos-username and then your Kerberos password in the password field. Note that you must add <span style=\"color: blue;\">ad\\<\/span> in front of your username.<\/li>\n<li><strong>600<\/strong> NMR: map a network drive to <span style=\"color: blue;\">\\\\casfs.bu.edu\\cic_b600<\/span> (there is an underscore between cic and b600) . You will be asked to login: in the username field enter AD\\your-BU-Kerberos-username and then your Kerberos password in the password field. Note that you must add <span style=\"color: blue;\">ad\\<\/span> in front of your username.<\/li>\n<\/ol>\n<h4 style=\"color: blue;\">Mac:<\/h4>\n<ol>\n<li>Open a Finder window, click Go and select Connect to server<\/li>\n<li><strong>400 NMR<\/strong>: map a network drive to <span style=\"color: blue;\">smb:\/\/casfs.bu.edu\/cic v400<\/span> (there is a space between cic and v400) . You will be asked to login: in the username field enter AD\\your-BU-Kerberos-username and then your Kerberos password in the password field. Note that you must add <span style=\"color: blue;\">ad\\<\/span> in front of your username.<\/li>\n<li><strong>500 NMR<\/strong>: map a network drive to <span style=\"color: blue;\">smb:\/\/casfs.bu.edu\/cic m500<\/span> (there is a space between cic and m500) . You will be asked to login: in the username field enter AD\\your-BU-Kerberos-username and then your Kerberos password in the password field. Note that you must add <span style=\"color: blue;\">ad\\<\/span> in front of your username.<\/li>\n<li><strong>600NMR<\/strong>: map a network drive to <span style=\"color: blue;\">smb:\/\/casfs.bu.edu\/cic_b600<\/span> (there is an underscore between cic and b600) . You will be asked to login: in the username field enter AD\\your-BU-Kerberos-username and then your Kerberos password in the password field. Note that you must add <span style=\"color: blue;\">ad\\<\/span> in front of your username.<\/li>\n<\/ol>\n<p>NOTE: Data that is on the CASFS shares are periodically archived into <span style=\"color: blue;\">\\\\casfs.bu.edu\\CIC Archive<\/span>. Once data is archived, they are deleted from the instrument data shares. If you can not find old data in your regular folders please connect to the CIC Archive share. All the data are stored as zip files. If you need help find your data contact Paul Ralifo at ralifo@bu.edu.<\/p>\n<h3>TEACHING NMR in SCI 346: Bruker Fourier 300 NMR (b300f)<\/h3>\n<p>For Windows users: map a network drive to <span style=\"color: blue;\">\\\\casfs.bu.edu\\cic_b300f<\/span> (there is an underscore between cic and b300f) . You will be asked to login: in the username field enter AD\\your-BU-Kerberos-username and then your Kerberos password in the password field. Note that you must add <span style=\"color: blue;\">ad\\<\/span> in front of your username.<\/p>\n<p>For Mac users: map a network drive to <span style=\"color: blue;\">smb:\/\/casfs.bu.edu\/cic_b300f<\/span> (there is an underscore between cic and b300f) . You will be asked to login: in the username field enter AD\\your-BU-Kerberos-username and then your Kerberos password in the password field. Note that you must add <span style=\"color: blue;\">ad\\<\/span> in front of your username.<\/p>\n<h4>Note, You must be connected to the network in one of the following ways:<\/h4>\n<ul>\n<li>Via ethernet cable on the Chemistry side of Metcalf\/SCI, in a Chemistry\/CMLD lab in LSE, or in a Chemistry lab in Photonics.<\/li>\n<li>Via the 802.1x wireless network.<\/li>\n<li>Via the on-campus VPN.<\/li>\n<li>Via the <a href=\"https:\/\/www.bu.edu\/tech\/services\/cccs\/remote\/vpn\/\">off-campus VPN<\/a>. (This is the only one that will work away from BU.)<\/li>\n<li>Via an Ethernet cable from ResNet locations.<\/li>\n<li>At a machine in the BU Common @ Mugar library.<\/li>\n<\/ul>\n<p>For general instructions on how to connect to a server, please see <a href=\"https:\/\/www.bu.edu\/casit\/information\/file-servers\/\">https:\/\/www.bu.edu\/casit\/information\/file-servers\/<\/a>.<\/p>\n<h3>When Publishing Peer-review Papers:<\/h3>\n<h4>For the Experimental:<\/h4>\n<p>The <sup>1<\/sup>H NMR and <sup>13<\/sup>C NMR spectra were recorded at 117.42 kG (<sup>1<\/sup>H 500 MHz, <sup>13<\/sup>C 125 MHz), 93.94 kG (<sup>1<\/sup>H 400 MHz, <sup>13<\/sup>C 100 MHz), or 70.50 kG (<sup>1<\/sup>H 300 MHz, <sup>13<\/sup>C 75 MHz) at ambient temperature as noted. Hydrogen chemical shifts are expressed in parts per million (ppm) relative to the residual protio solvent resonance: CDCl<sub>3<\/sub> \u03b4 7.24, DMSO-d6 \u03b42.50. For <sup>13<\/sup>C spectra, the center line of the solvent signal was used as internal reference: CDCl<sub>3<\/sub> \u03b4 77.16, DMSO-d6 \u03b4 39.52. Unless otherwise noted, each carbon resonance represents a single carbon (relative intensity). Inverse gated decoupled spectra using 5xT1 second delays between transients were used for carbon resonance integration to establish intensities greater than 1 carbon when not obvious. Multiplicities of <sup>13<\/sup>C NMR peaks were determined using HSQC, DEPT or APT spectra.<\/p>\n<h4>For the Acknowledgements:<\/h4>\n<p>We are grateful to the National Science Foundation for the purchase of the NMR\u2019s (CHE0619339) used in this work.<\/p>\n<\/div>\n","protected":false},"excerpt":{"rendered":"<p>NMR Data Access NOTE: if accessing from off campus you must connect via BU&#8217;s off-campus VPN. 1. All the CIC NMR data is being saved directly to the casfs.bu.edu server. Each instrument has its own share on the server. On the NMR host computers, the data will appear on the shares that were mounted as [&hellip;]<\/p>\n","protected":false},"author":10766,"featured_media":0,"parent":20,"menu_order":4,"comment_status":"closed","ping_status":"closed","template":"","meta":[],"_links":{"self":[{"href":"https:\/\/sites.bu.edu\/cheminst\/wp-json\/wp\/v2\/pages\/216"}],"collection":[{"href":"https:\/\/sites.bu.edu\/cheminst\/wp-json\/wp\/v2\/pages"}],"about":[{"href":"https:\/\/sites.bu.edu\/cheminst\/wp-json\/wp\/v2\/types\/page"}],"author":[{"embeddable":true,"href":"https:\/\/sites.bu.edu\/cheminst\/wp-json\/wp\/v2\/users\/10766"}],"replies":[{"embeddable":true,"href":"https:\/\/sites.bu.edu\/cheminst\/wp-json\/wp\/v2\/comments?post=216"}],"version-history":[{"count":30,"href":"https:\/\/sites.bu.edu\/cheminst\/wp-json\/wp\/v2\/pages\/216\/revisions"}],"predecessor-version":[{"id":614,"href":"https:\/\/sites.bu.edu\/cheminst\/wp-json\/wp\/v2\/pages\/216\/revisions\/614"}],"up":[{"embeddable":true,"href":"https:\/\/sites.bu.edu\/cheminst\/wp-json\/wp\/v2\/pages\/20"}],"wp:attachment":[{"href":"https:\/\/sites.bu.edu\/cheminst\/wp-json\/wp\/v2\/media?parent=216"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}